EPRW 2024 Recent Developments of Micro-SPE for Pesticides Analysis

Recent Developments of Micro-SPE for Pesticides Analysis

PAL µSPE Cartridge: A Greener Approach to Sample Prep

The PAL µSPE Cartridge aligns with Green Analytical Chemistry principles by minimizing solvent consumption and waste generation. Its miniaturized format and optimized design reduce the need for large solvent volumes, contributing to a more sustainable and eco-friendly laboratory environment.

Discover how the seamless integration of our PAL System and the new PAL µSPE Cartridges streamlines your laboratory processes, delivering unparalleled efficiency, accuracy, and reproducibility.

Don't miss Dr. Hans-Joachim Hübschmann's vendor talk on combining Quechers with micro-SPE for streamlined pesticide analysis.

Session Slot: V-7
Session Time: Wednesday, 18 September 2024; 14:10 – 14:45
Session Room: Room Fortran; Second Floor

Key functionality:

Septumless cartridge designs with patented sealing
High pressure rating (up to 10 bar)
Multiple elutions supported
Sorbent capacity: up to 100 mg packing possible
Chemically inert materials used
Free of extractables & leachables
Designed to penetrate pre-slit septa of vials
Designed to elute directly into PAL System liquid injection ports

More about the comparison µSPE to classical SPE

PAL System μSPE Cartridge Selection Guide with Publications

Cartridges	Pesticides Residue Analysis	Application Information	Publications
uSPE-GCQuE1-45-V PAL System μSPE Cartridge GC QuEChERS sorbent mix 1, 45 mg [C18, PSA, MgSO4, GCB] 108 pcs type 01-05B		µSPE Cartridge for GC amenable pesticides. Follows AOAC 2007.01 and EN 15662 methodology.	Steven Lehotay et al, 2022 https://doi.org/10.1016/j.chroma.2022.463596 Amadeo Fernandez-Alba et al. 2023, open Access https://doi.org/10.1016/j.chroma.2023.463906 Mette Poulson et al., 2021, open Access https://doi.org/10.1016/j.chroma.2021.462384 Fully Automated QuEChERS Extraction and Clean-up of Organophosphate Pesticides in Orange Juice, Hübschmann et al, 2023 Performance Qualification Test for PAL System µSPE GC QuEChERS-45-V Cartridges
uSPE-GCQuE2-44-V PAL System μSPE Cartridge GC QuEChERS sorbent mix 2, 44 mg [C18, PSA, MgSO4] 108 pcs type 01-19A		µSPE Cartridge without Carbon for GC amenable pesticides. Follows AOAC 2007.01 and EN 15662 methodology.	Steven Lehotay et al, 2022 https://doi.org/10.1016/j.chroma.2022.463596 Amadeo Fernandez-Alba et al. 2023, open Access https://doi.org/10.1016/j.chroma.2023.463906 Mette Poulson et al., 2021, open Access https://doi.org/10.1016/j.chroma.2021.462384 Fully Automated QuEChERS Extraction and Clean-up of Organophosphate Pesticides in Orange Juice, Hübschmann et al, 2023 Performance Qualification Test for PAL System µSPE GC QuEChERS-45-V Cartridges
uSPE-GCQuE3-45-V PAL System μSPE Cartridge GC QuEChERS sorbent mix 3, 45 mg [PSA, MgSO4] 108 pcs type 01-14A		µSPE Cartridge for GC amenable pesticides in low fat matrices. Follows AOAC 2007.01 and EN 15662 methodology.
uSPE-LC-QuE1-30-T PAL System μSPE Cartridge LC & GC QuEChERS sorbent mix, 30 mg [C18, Z-Sep, GCB] 96 pcs in blister type 01-03A		μSPE Cartridge for pesticides in complex spice matrixes	Goon et al: Journal of AOAC International Vol. 103, No.1, 202 https://doi.org/10.5740/jaoacint.19-0202 Performance Qualification Test for PAL System µSPE LC QuEChERS-30-T Cartridges
uSPE-SAX-50-V PAL System μSPE Cartridge Strong Anion Exchange (SAX), 50 mg for polar, anionic pesticides or other anionic compounds 108 pcs type 01-20A		µSPE Cartridge for LC amenable pesticides. ollows AOAC 2007.01 and EN 15662 methodology.	Analysis of Highly Polar Pesticides - Automated Micro-SPE Clean-up of Complex Food Matrices for LC-MS/MS Florencia Jesús , Amadeo Rodríguez Fernández-Alba, Hans-Joachim Hübschmann

Methods and Installation Guides for automated PAL System µSPE clean-up of QuEChERS extracts

We offer various methods (scripts) for an automated µSPE clean-up of QuEChERS extracts with a subsequent liquid injection.
In order to access our scripts, installation guides and recent publications, we ask you to provide some information e.g. the serial number of your device.

After filling in the corresponding fields you will be automatically forwarded to the download area.

Cartridges	Application	Methods, Installation Guides & recent publications
Cartridges	Application	CDS	FW Version
uSPE-GCQuE1-45-V PAL System µSPE Cartridge GC QuEChERS sorbent mix 1, 45 mg [C18, PSA, MgSO4, GCB] 108 pcs type 01-05B	µSPE Cartridge for GC amenable pesticides. Follows AOAC 2007.01 and EN 15662 methodology.	MassHunter OpenLab	Script and Installation Guide AGI for FW 2.4 - 3.x Script and Installation Guide AGI for FW 4.x
		Xcalibur Chromeleon	Script and Installation Guide TMO for FW 2.4 - 3.x Script and Installation Guide TMO for FW 4.x
		GCMSsolution	Script and Installation Guide SHIM for FW 2.4 - 3.x
		Empower 3 Sciex OS Hystar	Script and Installation Guide Others for FW 2.4 - 3.x Script and Installation Guide Others for FW 4.x
uSPE-GCQuE2-44-V PAL System µSPE Cartridge GC QuEChERS sorbent mix 2, 44 mg [C18, PSA, MgSO4] 108 pcs type 01-19A	µSPE Cartridge without Carbon for GC amenable pesticides. Follows AOAC 2007.01 and EN 15662 methodology.	MassHunter OpenLab	Script and Installation Guide AGI for FW 2.4 - 3.x Script and Installation Guide AGI for FW 4.x
		Xcalibur Chromeleon	Script and Installation Guide TMO for FW 2.4 - 3.x Script and Installation Guide TMO for FW 4.x
		GCMSsolution	Script and Installation Guide SHIM for FW 2.4 - 3.x
		Empower 3 Sciex OS Hystar	Script and Installation Guide Others for FW 2.4 - 3.x Script and Installation Guide Others for FW 4.x
uSPE-GCQuE3-45-V PAL System µSPE Cartridge GC QuEChERS sorbent mix 3, 45 mg [PSA, MgSO4] 108 pcs type 01-14A	µSPE Cartridge for GC amenable pesticides in low fat matrices. Follows AOAC 2007.01 and EN 15662 methodology	MassHunter OpenLab	Script and Installation Guide AGI for FW 2.4 - 3.x Script and Installation Guide AGI for FW 4.x
		Xcalibur Chromeleon	Script and Installation Guide TMO for FW 2.4 - 3.x Script and Installation Guide TMO for FW 4.x
		GCMSsolution	Script and Installation Guide SHIM for FW 2.4 - 3.x
		Empower 3 Sciex OS Hystar	Script and Installation Guide Others for FW 2.4 - 3.x Script and Installation Guide Others for FW 4.x
uSPE-LC-QuE1-30-T PAL System µSPE Cartridge LC & GC QuEChERS sorbent mix, 30 mg [C18, Z-Sep, GCB] 96 pcs in blister type 01-03A	µSPE Cartridge for LC amenable pesticides. Follows AOAC 2007.01 and EN 15662 methodology.	Sciex Analyst	Script and LC Installation Guide Others for FW 2.4 - 3.x
uSPE-Sax-50-V PAL System µSPE Cartridge Strong Anion Exchange (SAX), 50 mg 108 pcs type 01-20A	µSPE Cartridge for polar, anionic pesticides or other anionic compounds	Offline	Script and Installation Guide for FW 2.4 - 3.x