uSPE-LCQuE1-30-T
PAL3-TH-D857-uSPE
PAL3-WashFast
PAL3-Rack-Cart-uSPE54
PAL3-Rack-Cart-uSPE96
PAL3-Rack-Cart-uSPE96-B
Vial-0.3-ND9-PP-100
Vial-1.5-ND9-CG-100
Cap-ND9-PP-SP10S-100
Cap-ND9-St-SP10Sb-100
PAL3-HW-uSPE54
PAL3-Vial-Lock-uSPE54
PAL3-Wasterecept-uSPE
uSPE-FILT-V
uSPE-GCB-10-V
uSPE-GCQuE1-45-V
uSPE-GCQuE2-44-V
uSPE-GCQuE3-45-V
uSPE-LCQuE1-30-T
uSPE-SAX-50-V
uSPE-WAX-50-V
PAL Systems for uSPE / QuEChERS cleanup
ASMS 2025 - Streamlined Analysis of Polar and Non-Polar Metabolites in Plasma Using Automated Micro-SPE LC/MS
This poster presents two use cases for streamlined lipid profiling in plasma using automated Micro Solid Phase Extraction (μSPE). Where the workflows on NIST (SRM 1950) plasma samples was tested, with spiked internal standard (Ultimate SPLASH ONE) and optimized the extraction and elution parameters. Briefly, it focused on two cartridge sorbent types Mixed-Mode Cation Exchange (MCX) and C18 (CEC) and showcased their usage.
ASMS 2025 - Fully automated implementation of EPA Method 1633 for LC-MS/MS analysis of PFAS in environmental samples using a customized robotic autosampler
ASMS 2025 - Fully Automated Workflow for Volatile PFAS Analysis in Food Contact Materials Using GC-Triple Quadrupole
Gas Chromatography coupled with Triple Quadrupole Mass Spectrometry (GC/TQ) offers a robust and sensitive method for
detecting volatile PFAS. However, manual sample preparation could pose a bottleneck, impacting lab productivity. This study presents a robust and fully automated method using the PAL3 platform with GC/TQ for quantifying more than 30 volatile PFAS in FCMs, such as paper coffee cups. The automation approach minimizes human error, improving reliability
and reproducibility for routine analysis and safety assessments of PFAS in FCMs.
Sample Preparation Compendium
Automated, Green, and Efficient
A Compendium on Micromethods in Analytical Sample Preparation
Discover robust, precise, and reliable analytical methods while following the principles of Green Analytical Chemistry in various fields such as Food & Food Safety, Environmental, Clinical, Life Science, and Chemical.
The Power of Micro Solid Phase Extraction
This eBook explores the potential of uSPE to transform analytical workflows. It highlights the key benefits of uSPE, compares it with traditional techniques and examines its application across various industries. This resource provides a comprehensive guide for scientists and lab managers looking to optimize their sample preparation processes, achieve higher precision and embrace sustainable practices in analytical chemistry.
Advancing PFAS Analysis - Robotic Automation and Streamlined LC/MS Workflows
To support the scientific community and advance PFAS analysis we are proud to offer a webinar on this topic.
Key topics:
Advantages of automated and miniaturized uSPE clean-up in pesticides residues analysis
Recent developments in pesticides analysis extend the well-established methods to higher productivity and reliability while minimizing consumption and exposition to harmful chemicals. A workflow was developed that allows automatic preparation of calibration standards, automatic sample dilution, and automatic clean-up of sample extracts on one instrument, showing that miniaturized automated solutions are reducing errors, improving analytical consistency and protecting the environment in one convenient approach.
Presented by:
Thomi Preiswerk, Senior Account Manager, CTC Analytics AG
Gwen Lim , Specialist for automated sample preparation, CTC Analytics
Ederina Ninga, Postdoc, Research Group for Analytical Food Chemistry, Danish Technical University
Automated Sample Preperation for LC/MS and GC/MS - Solutions for Food and Environmental Analysis
In this presentation we want to discuss an important development and a demand from analytical laboratories about the standardization and the automation of sample preparation procedures for food safety, environmental, the forensic or pharmaceutical analysis.
Presented by:
Hans-Joachim Huebschmann, PhD
High-Sensitivity PFAS Determination in Seafood
This application note showcases a fully automated workflow for the precise quantification of 73 PFAS in seafood. Utilizing a PAL RTC autosampler and Agilent triple quadrupole LC/MS system (LC/TQ), the method automates calibration, QuEChERS extraction, and μSPE clean-up.
Analysis of Highly Polar Pesticides
Micro-SPE (uSPE) emerged as an automated green micromethod for sample preparation and clean-up in food safety, proteomics, forensic, environmental and analysis since more than ten years. Applications are wideranging and cover drugs, environmental contaminants, and, in particular, the extract clean-up in multiresidue pesticide analysis. The automation of the uSPE sample preparation steps led to the desired standardization of the applied sorbent materials for extract clean-up for the large variety of food commodities, an increase in sample throughput, and the welcome potential for offline and online hyphenation with GC/MS, LC/MS or even IC analysis.
Fully Automated QuEChERS Extraction and µSPE Clean-up of Organophosphate Pesticides in Orange Juice
Chiew Mei Chong1, Hans-Joachim Hübschmann2
1 CTC Analytics Pte. Ltd., Singapore.
2 HANS Analytical Solutions, Osaka, Japan.
