SPME Arrow - Trace Level sensitivity and Improved Mechanical Stability

Smart SPME Arrow - New Dimension for Solid Phase Micro-Extraction

Superior Sensitivity and Improved Mechanical Stability

The PAL Smart SPME Arrow is a new patented technology for micro-extraction combining trace level sensitivity with high mechanical robustness.

Key functionality of Smart SPME Arrows:

Available in 1.1 mm (red body) or 1.5 mm (yellow body) outer diameter
Smart SPME Arrow 1.5 mm - for use with solvents or reagents, that may lead to moderate swelling of PDMS phases
5 coating materials and 2 different film thicknesses
Arrow-shaped tip allows smooth vial penetration and injector septa
Design fully protects the coating material
Color coded to indicate SPME Arrow coating and film thickness
Integrated holder design facilitates installation and maintenance

Benefits compared to classical SPME Fibers:

Up to 10 x more sensitivity compared to classical SPME
Up to 5 x longer lifetime
Full traceability thank to smart technology
Designed for headspace and immersion sampling

*Widesleeve arrows with 1.5mm diameter have the same phase dimensions as the corresponding 1.1mm Arrows. The space to the outer needle allows phase swelling for special applications i.e. with high amounts of organic solvents. For all standard
applications with aqueous samples we recommend to use 1.1mm Arrows.

Smart SPME Arrow Selection Guide

Detailed information on the specifications and handling of Smart SPME Arrows are available. For automation of SPME Arrow with the PAL RCT and PAL RSI a SPME Arrow Starter Kit is available, as well as an Agitator module for agitation/sample Enrichment at up to 200°C, SPME Arrow conditioning module and a Heatex Stirrer module.

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The PAL Smart SPME Arrows are available in order quantities of one, three or five Smart SPME Arrows per box.
For method development, a set of each fiber type (set of five) is available.

PAL Smart SPME Arrows work with all the PAL3 Systems, however to use the smart capabilities (ID, traceability, usage history) the PAL3 Series II System is required.

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Application Notes

Profiling of Gin Botanicals by Headspace-SPME-ARROW-GCxGC-MSD/FID

Gins are essentially neutral spirits flavoured with various botanicals by compounding or by distillation. The combination of HS-SPME Arrow with GCxGC-MSD/FID is a very powerful tool in the comparative analysis of samples with complex matrices.

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Rice flavor compounds from robotically cooked rice

Application Notes

Rice flavor compounds from robotically cooked rice

Here we present a facile and robust method how to boil and then analyze rice samples in a fully automated fashion.

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PAL Smart SPME Arrow

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Care & User (handling) Guides

PAL Smart SPME Arrow

General Information for PAL Smart SPME Arrows

PAL Ingenious News

PAL Ingenious News April 2021

Drinking Water Quality Control - Screening for 57 Odorous Substances using SPME Arrow
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Fully Automated Analysis of E-Cigarette Juice

Posters

Fully Automated Analysis of E-Cigarette Juice

Static headspace for the main volatiles and HS-SPME extraction are combined in one workflow for comprehensive analysis of main and trace components.

Posters

Robustness of SPME Arrow Immersion Sampling

Fully automated SPME Arrow immersion technique with GC/MS analysis is an excellent option to analyze PAH compounds in drinking water; with higher throughput and robustness

Solid phase microextraction (SPME) - How does it work for my samples?

Webinars

Solid phase microextraction (SPME) - How does it work for my samples?

This webinar offers a close insight into the operation and latest developments of automated SPME for VOCs and SVOCs by headspace, direct immersion and derivatization techniques. Key applications for food, water, environmental and forensic samples for use in every laboratory for GC-MS and LC-MS, also direct MS analysis are discussed.

Presented by:
Hans-Joachim Huebschmann, PhD

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Flavor and Off-Flavor Analysis using Solid Phase Microextraction

Webinars

Flavor and Off-Flavor Analysis using Solid Phase Microextraction

Solid Phase Micro-Extraction (SPME) is widely used for chemical analysis of foods, beverages and food contact materials. As an automated technique, the SPME applications are selected for their simplicity, throughput and extraction efficiency. As a solvent-free extraction, it is gains even more importance today as a green analytic technique. Besides the traditional SPME Fiber, the new SPME Arrow is enhancing trace level sensitivity at high mechanical robustness. With these features, this presentation will give insight on SPME analysis in coffee, wine and off-flavors.

Presented by:

Erich Leitner, Graz University of Technology Institute of Analytical Chemistry and Food Chemistry

Stefan Cretnik, PhD, Product Manager, CTC Analytics AG

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