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Sample Preparation Compendium

Automated, Green, and Efficient
A Compendium on Micromethods in Analytical Sample Preparation

Discover robust, precise, and reliable analytical methods while following the principles of Green Analytical Chemistry in various fields such as Food & Food Safety, Environmental, Clinical, Life Science, and Chemical.

Headspace Analysis: Reproducibility of Syringe Headspace Injections for Aqueous Samples

Application Notes

Headspace Analysis: Reproducibility of Syringe Headspace Injections for Aqueous Samples

This article describes the optimization of residual solvents analysis according USP <467> and Ph.Eur. 2.4.24 using the automated syringe headspace technique on GC-FID and GC-MS systems. The precision of analysis ranged from 4.3 to 7.8 % RSD (GC-FID) for class 2 solvents for all analytes investigated in this study. These values fully comply with USP <467> and Ph. Eur. 2.4.24 requirements.

The Power of Micro Solid Phase Extraction

eBooks

The Power of Micro Solid Phase Extraction

This eBook explores the potential of μSPE to transform analytical workflows. It highlights the key benefits of μSPE, compares it with traditional techniques and examines its application across various industries. This resource provides a comprehensive guide for scientists and lab managers looking to optimize their sample preparation processes, achieve higher precision and embrace sustainable practices in analytical chemistry.

High-Sensitivity PFAS Determination in Seafood

Application Notes

High-Sensitivity PFAS Determination in Seafood

This application note showcases a fully automated workflow for the precise quantification of 73 PFAS in seafood. Utilizing a PAL RTC autosampler and Agilent triple quadrupole LC/MS system (LC/TQ), the method automates calibration, QuEChERS extraction, and μSPE clean-up.

Trace-level Volatile Organic Pollutants in Water

Application Notes

Trace-level Volatile Organic Pollutants in Water

This application note demonstrates the analysis of tracelevel volatile organic compounds (VOCs) in water using
an automated headspace-trap GC/MS workflow.
• Ultra-low detection limits (ppt) for confident quantitation of VOCs.
• Exceptional linearity and precision for accurate and reliable results.
• High performance exceeding regulatory standards for water quality.

Technical Information / Specifications

Specifications PAL RTC / RSI including Series II (LC & GC)

Automated MALDI-TOF MS Workflows for Streamlined Bacterial Identification

Application Notes

Automated MALDI-TOF MS Workflows for Streamlined Bacterial Identification

This application note demonstrates the successful automation of two sample preparation workflows, Formic Acid (FA) and Beads method, for bacterial identification using Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry (MALDI-TOF MS).